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As a end result, S-CoOOH exhibits an overpotential of 226 mV at 10 mV cm-2, which is 148 mV decrease than that of R-CoOOH. Such a high-spin state Co3+ digital configuration could lead to extra electronic states across the Fermi degree. C Normalized O K-edge XAS spectra (the inset exhibits the enlarged results of S-CoOOH within pre-edge round 531 to 533 eV). B Normalized Co K-edge XAS spectra (the inset reveals the enlarged outcome within white line round 7727 to 7732 eV). These oxygen vacancies resulting from bond breakage, would concurrently bring coordinatively unsaturated Co and O atoms.
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